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Kühne, Irina A, Mereacre, Valeriu, Anson, Christopher E, Powell, Annie K
Chemical communications (Cambridge, England), 18 January 2016, Vol.52(5), pp.1021-4
[Peer Reviewed Journal]
MEDLINE/PubMed (U.S. National Library of Medicine)
Title: Microwave-Mediated Synthesis of Bulky Lanthanide Porphyrin–Phthalocyanine Triple-Deckers: Electrochemical and Magnetic Properties Author:Jin, Hong-Guang; Jiang, Xiaoqin; Kühne, Irina A; Clair, Sylvain; Monnier, Valérie; Chendo, Christophe; Novitchi, Ghenadie; Powell, Annie K; Kadish, Karl M; Balaban, Teodor Silviu Subject:Chemical Sciences ; Coordination Chemistry ; Chemistry Description:
Five heteroleptic lanthanide porphyrin−bis-phthalocyanine triple-decker complexes with bulky peripheral groups were prepared via microwave-assisted synthesis and characterized in terms of their spectroscopic, electrochemical, and magnetic properties. These compounds, which were easily obtained under our preparative conditions, would normally not be accessible in large quantities using conventional synthetic methods, as a result of the low yield resulting from steric congestion of bulky groups on the periphery of the phthalocyanine and porphyrin ligands. The electrochemically investigated triple-decker derivatives undergo four reversible one-electron oxidations and three reversible one-electron reductions. The sites of oxidation and reduction were assigned on the basis of redox potentials and UV−vis spectral changes during electron-transfer processes monitored by thin-layer spectroelectrochemistry, in conjunction with assignments of electronic absorption bands of the neutral...
Is part of:
Inorganic chemistry, 2017, Vol.56(9), pp.4864-4873
Identifier:
0020-1669 (ISSN); 1520-510X (E-ISSN); 10.1021/acs.inorgchem.6b03056 (DOI)
Kühne, Irina A, Magnani, Nicola, Mereacre, Valeriu, Wernsdorfer, Wolfgang, Anson, Christopher E, Powell, Annie K
Chemical communications (Cambridge, England), 21 February 2014, Vol.50(15), pp.1882-5
[Peer Reviewed Journal]
MEDLINE/PubMed (U.S. National Library of Medicine)
Kühne, Irina A, Kostakis, George E, Anson, Christopher E, Powell, Annie K
Chemical communications (Cambridge, England), 14 February 2015, Vol.51(13), pp.2702-5
[Peer Reviewed Journal]
MEDLINE/PubMed (U.S. National Library of Medicine)